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Special modified phenolic resin manufacturing method
1. Introduction
Special modified phenolic resin is an important chemical production raw materials, with excellent heat resistance, corrosion resistance, electrical insulation and mechanical properties, widely used in composite materials, abrasives, refractory materials, insulating materials and other fields. This article will detail the manufacturing method of special modified phenolic resin.
2. raw materials and equipment
1. raw materials: phenol, formaldehyde, modifier (such as ethylenediamine, glycerol, etc.), catalyst (such as hydrochloric acid, sodium hydroxide, etc.).
2. Equipment: reaction kettle, stirrer, thermometer, pH meter, condenser, vacuum pump, etc.
3. Manufacturing Steps
1. Ingredients: According to a predetermined formula, phenol, formaldehyde, modifier and catalyst are added to the reactor in proportion.
2. Stirring and heating: turn on the stirrer to fully mix the raw materials, and heat the reactor at the same time to control the reaction temperature within an appropriate range.
3. Reaction: When the temperature in the reaction kettle reaches the preset value, keep the constant temperature, let the raw materials fully react, and generate special modified phenolic resin.
4. Post-treatment: After the reaction, the product is post-treated, such as cooling, filtering, drying, etc., to obtain the final special modified phenolic resin product.
Precautions for
4.
1. Strictly control the ratio of raw materials and reaction temperature to ensure the performance and stability of the product.
2. Select appropriate modifiers and catalysts according to needs to achieve the special properties of the product.
3. In the reaction process, it is necessary to pay close attention to the changes of temperature and pH value in the reactor and adjust the process parameters in time.
4. In the post-treatment process, ensure that the product is fully cooled, filtered and dried to improve product quality.
5. Quality Testing and Analysis
1. Quality testing of special modified phenolic resin products, including appearance, viscosity, solid content, pH value and other indicators.
2. The structure and performance of the product were analyzed by infrared spectroscopy, thermogravimetric analysis and scanning electron microscope.
6. waste treatment and environmental protection measures
1. Classify the waste generated in the production process, such as recyclable waste for recycling and safe disposal of hazardous waste.
2. Strengthen the treatment of pollutants such as waste gas, waste water and noise in the production process to ensure that they meet the discharge standards.
3. Improve the environmental awareness of employees, strengthen environmental training and operating standards, and ensure that the production process meets environmental requirements.
7. safety production and protective measures
1. Strictly implement safety production rules and regulations to ensure the normal operation and maintenance of production equipment.
2. Provide safety training to employees to improve their safety awareness and operation skills.
3. In the production process, equipped with corresponding safety protection facilities and equipment, such as fire prevention equipment, gas masks, etc., to ensure the personal safety of employees.
8. Conclusion
special modified phenolic resin manufacturing method involves many links and matters needing attention, need to strictly control the proportion of raw materials, reaction temperature and post-treatment process and other parameters, in order to ensure product quality and performance. At the same time, strengthen environmental protection and safety management in the production process, improve production efficiency, reduce production costs, and create greater economic and social benefits for enterprises.