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The manufacturing method
of bisphenol A polyoxypropylene ether series
1. Introduction
bisphenol A polyoxypropylene ether series is an important raw material for the production of chemical products, which is widely used in coatings, inks, cleaning agents, plastic processing aids and other fields. Due to its unique chemical properties and wide range of applications, the manufacturing methods of bisphenol A polyoxypropylene ether series have attracted much attention. This article will introduce the manufacturing method of bisphenol A polyoxypropylene ether series in detail, including raw material preparation, polymerization reaction, post-treatment and other processes.
2. Raw Material Preparation
The production of the bisphenol A polyoxypropylene ether series requires preparation of the following raw materials: bisphenol A, propylene oxide, catalyst, solvent, etc. Among them, bisphenol A and propylene oxide are the main reactants, the catalyst is used to promote the polymerization reaction, and the solvent is used to adjust the viscosity of the reaction system.
3. Polymerization
The key step in the manufacture of
bisphenol A polyoxypropylene ether series is polymerization. The specific steps are as follows:
1. adding bisphenol A and a catalyst into a reaction kettle and heating to a certain temperature.
2. Gradually add propylene oxide dropwise, while controlling the reaction temperature and pressure, so that propylene oxide and bisphenol A ring-opening polymerization reaction.
3. After the addition is completed, continue to heat the reaction for a certain period of time, so that the molecular chain fully growth.
4. post-treatment
After the polymerization reaction is completed, post-treatment is required to obtain high-quality bisphenol A polyoxypropylene ether products. The specific steps are as follows:
1. cooling the reaction kettle, pouring the reaction solution into a separatory funnel, and washing with water to remove the catalyst and unreacted raw materials.
2. After layering, pour out the upper aqueous solution, and filter the lower organic phase with a vacuum pump to remove water and impurities.
3. The obtained crude product is recrystallized with a solvent to obtain a higher purity bisphenol A polyoxypropylene ether product.
Precautions for
5.
1. During the polymerization reaction, the reaction temperature and pressure need to be strictly controlled to prevent the occurrence of side reactions and the decomposition of the product.
2. In the post-treatment process, it is necessary to fully wash and filter to ensure the quality of the product.
3. During the entire manufacturing process, you need to pay attention to safety and avoid contact with sensitive parts such as skin and eyes.
6. Conclusion The manufacturing method of
bisphenol A polyoxypropylene ether series includes raw material preparation, polymerization reaction and post-treatment. By strictly controlling the reaction conditions and post-treatment process, high-quality bisphenol A polyoxypropylene ether products can be obtained. The product has a wide range of application prospects and can provide important raw material support for coatings, inks, cleaning agents, plastic processing aids and other fields.