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The manufacturing method
of terephthalic ether
1. Introduction
terephthalic ether is an important chemical production raw material, widely used in polymers, pharmaceuticals, pesticides, spices and other fields. Due to its unique chemical properties and wide range of applications, the manufacturing method of terephthalic ether has attracted much attention. This article will introduce the manufacturing method of terephthalic ether in detail, including raw material preparation, reaction process, post-treatment and so on.
2. Raw Material Preparation
The main raw materials for manufacturing terephthalic ether are phenol and methanol. In order to ensure the smooth progress of the reaction, it is necessary to purify the phenol and methanol to remove the water and impurities.
3. Reaction Process
The manufacturing process of terephthalic ether mainly includes the following steps:
1. Phenol and methanol are esterified under the action of acidic catalyst to generate phenol methyl ester. Commonly used acidic catalysts include sulfuric acid, hydrochloric acid, and the like.
2. Phenol methyl ester is etherified with methanol in the presence of an alkaline catalyst to produce terephthalic ether. Commonly used basic catalysts include sodium hydroxide, potassium hydroxide, and the like.
In the above two steps, attention should be paid to controlling the reaction temperature, reaction time and the amount of catalyst to ensure the smooth progress of the reaction and the purity of the product.
4. post-treatment
After the end of the
reaction, the product needs to be post-treated, including distillation, washing, drying and the like, to obtain pure terephthalic ether.
5. precautions
In the process of manufacturing terephthalic ether, the following matters need to be paid attention to:
1. Strictly control the reaction temperature and time to avoid the formation of by-products.
2. Select the appropriate catalyst and control its dosage to ensure the efficiency of the reaction and the purity of the product.
3. In the post-treatment process, care should be taken to avoid decomposition and pollution of the product.
6. Conclusion The manufacturing method of
terephthalic ether includes the steps of raw material preparation, reaction process and post-treatment. By strictly controlling the reaction conditions and selecting a suitable catalyst, high purity terephthalic ether can be obtained. The compound has a wide range of applications in the field of chemical industry, so it is of great significance to study its manufacturing methods.