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The manufacturing method
of dysprosium oxide
1. Introduction
dysprosium oxide is an important chemical raw material, widely used in high-tech fields, such as laser materials, fluorescent powder, magnetic materials, etc. With the continuous development of science and technology, the demand for dysprosium oxide is gradually increasing. Therefore, it is of great significance to study the manufacturing method of dysprosium oxide for improving production efficiency, reducing costs and improving product quality. This article will introduce the manufacturing method of dysprosium oxide, including raw material preparation, reaction process, post-treatment and so on.
2. raw material preparation
manufacturing dysprosium oxide is the main raw material of rare earth element dysprosium compounds, such as dysprosium nitrate, dysprosium chloride. In the process of raw material preparation, it is necessary to ensure that the purity and particle size of the raw materials meet the requirements to avoid adverse effects on subsequent reactions. At the same time, it is also necessary to carry out strict quality inspection on the raw materials to ensure that the raw materials do not contain harmful impurities.
3. reaction process
The manufacturing method of dysprosium oxide mainly uses chemical method, that is, the compound of dysprosium is converted into dysprosium oxide by chemical reaction. The specific reaction process is as follows:
1. add dysprosium nitrate or dysprosium chloride into a reaction kettle, add an appropriate amount of water, and adjust the pH value to the desired range.
2. At a certain temperature, an oxidizing agent, such as hydrogen peroxide or nitric acid, is added to oxidize the dysprosium compound to generate dysprosium oxide.
3. It is necessary to control the reaction temperature and pH value during the reaction to ensure the smooth progress of the reaction and the quality of the product.
4. After completion of the reaction, operations such as filtration and washing are carried out to obtain a crude dysprosium oxide.
4. post-treatment
dysprosium oxide crude products need to be post-treated to improve purity, improve particle size, remove impurities and other purposes. Specific post-treatment methods include:
1. washing: the crude dysprosium oxide is washed several times with pure water or acidic aqueous solution to remove impurities and ions on the surface.
2. Drying: The washed crude dysprosium oxide is dried to obtain a dried dysprosium oxide product.
3. Screening: According to product requirements, the dried dysprosium oxide product is screened to obtain a product that meets the particle size requirements.
5. precautions
In the manufacturing process of dysprosium oxide, the following matters need to be paid attention to:
1. Control the reaction temperature and pH value to ensure the smooth progress of the reaction and the quality of the product.
2. The purity and particle size of the raw materials need to meet the requirements to avoid adverse effects on subsequent reactions.
3. It is necessary to pay attention to safety during the manufacturing process and avoid contact with dysprosium oxide and other harmful substances.
4. In the post-processing process, it is necessary to ensure that the purity and particle size of the product meet the requirements to avoid affecting the use of the product.
6. Conclusion The manufacturing method of
dysprosium oxide mainly adopts chemical method, by controlling the reaction temperature and pH value and other conditions, the dysprosium compound is converted into dysprosium oxide. In the post-treatment process, washing, drying, sieving and other operations are required to improve the purity and particle size of the product. It is necessary to pay attention to safety and quality control in the manufacturing process to ensure product quality and reliability.