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Manufacturing method
of methyl cerate
methyl cerate is an important raw material for chemical production, which is widely used in plastics, rubber, coatings, inks and other fields. This article will introduce the manufacturing method of methyl cerate, including raw material preparation, esterification reaction, distillation and purification steps.
1. Raw Material Preparation
The main raw materials for the manufacture of methyl cerate are ceric acid and methanol. Waxy acids can be extracted from animal and vegetable oils and fats, and can also be prepared by chemical synthesis methods. Methanol is a common organic solvent and is commercially available.
2. esterification
esterification is a key step in the manufacture of methyl cerate. In the esterification reaction, ceric acid and methanol react to produce methyl cerate and water under the action of acidic catalyst. Commonly used acidic catalysts include sulfuric acid, hydrochloric acid, and the like.
esterification reaction is generally carried out under heating and refluxing conditions, the progress of the reaction can be promoted. During the reaction, it is necessary to constantly monitor the acidity and ester content of the reaction solution to determine the extent and end point of the reaction.
distillation purification
After the reaction is completed, the reaction solution needs to be distilled and purified to obtain methyl cerate with higher purity. Before distillation and purification, the catalyst and water in the reaction solution need to be removed to avoid the influence on the distillation process.
In the process of
distillation, it is necessary to select appropriate distillation conditions and equipment according to the physical properties such as the boiling point and vapor pressure of methyl cerate to ensure the purity and yield of the product.
Precautions for
4.
1. During the manufacturing process, you need to pay attention to safety to avoid accidents such as fire and explosion.
2. In the process of raw material preparation and reaction, it is necessary to strictly control the quality and proportion of raw materials to ensure the smooth progress of the reaction and the quality of the product.
3. In the process of distillation and purification, it is necessary to select appropriate distillation conditions and equipment to avoid product loss and quality degradation.
In short, the manufacturing method of methyl cerate requires certain chemical knowledge and skills, as well as safety and product quality. Only by mastering the correct manufacturing method can we produce high-quality methyl cerate and provide reliable raw material guarantee for chemical production.