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[Chemical Knowledge]：Clever operation, do acyl azide more handy

Read： 675 Time：8months ago Source：Transform the World with Simplicity

Acyl azide is an important organic synthesis reaction, which is widely used in medicine, pesticide, dye and other fields. In the acyl azide reaction, some important operation skills and safety precautions should be paid attention to to ensure the smooth progress of the experiment and the safety of the experimenter. The experimental conditions for

to do acyl azides are very important. When selecting a solvent, it is necessary to select a solvent that can effectively dissolve the reactants and is relatively mild to the reaction, such as dimethylformamide (DMF) or acetonitrile. In addition, it is necessary to strictly control the reaction temperature, and it is usually necessary to carry out the reaction at a low temperature in order to avoid the occurrence of side reactions. Safety issues in

reactions also require attention. Because the azide compound produced in the acyl azide reaction is highly explosive, it is necessary to pay attention to avoid generating static electricity and avoid exciting its explosive during operation. The tightness of the

reaction device also needs to be checked to avoid reactor explosion.

In addition, some basic experimental rules need to be observed during the operation, such as wearing laboratory clothes and goggles, keeping the operation area clean and tidy, and prohibiting individual operation. These are important guarantees to ensure the safety of the experiment and the smooth progress of the experiment.

In general, doing acyl azides requires strict mastery of experimental conditions and operating skills, and strict compliance with experimental codes, in order to make the experiment more handy. It is hoped that the introduction of this article will be helpful to everyone in the acyl azide reaction.

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