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Source:Transform the World with Simplicity
BDP (bisphenol A bis (diphenyl phosphate)) is a widely used flame retardant, mainly used in plastics and electronics. The following is the manufacturing method of BDP:
raw material preparation
1. Bisphenol A(BPA):BPA is the main raw material of BDP. It is a common chemical raw material and can be prepared from phenol and pyruvic acid.
2. Phosphorus chloride: Phosphorus chloride is a key raw material for the preparation of BDP and is usually produced by the reaction of phosphorus and chlorine.
reaction step
1. reaction of bisphenol A with phosphorus chloride: bisphenol A and phosphorus chloride are added into a reactor according to a certain molar ratio, and the reaction is carried out at a certain temperature and pressure. The reaction is exothermic and it is necessary to control the reaction temperature to avoid excessive reaction and formation of by-products.
2. Dehydration cyclization: After the reaction is completed, a dehydration cyclization reaction is required to generate BDP. This step needs to be carried out at an elevated temperature and usually requires the addition of a catalyst to facilitate the reaction.
3. Post-treatment: After the reaction is completed, the product needs to be post-treated, including washing, drying, crystallization and other steps, in order to obtain a higher purity BDP product.
precautions
1. Control the reaction temperature: Since the synthesis reaction of BDP is an exothermic reaction, it is necessary to control the reaction temperature to avoid safety accidents and the generation of by-products.
2. Selecting a suitable catalyst: The dehydration cyclization reaction requires the addition of a catalyst, and a suitable catalyst needs to be selected to improve the reaction efficiency and product purity.
3. Safety protection: Because the raw materials and products involved have certain toxicity, it is necessary to strengthen safety protection measures in the production process to ensure the health of production personnel.
The above is the manufacturing method of BDP. The specific production process and equipment need to be selected and designed according to the actual situation. At the same time, in order to ensure product quality and environmental protection, it is necessary to strictly control various parameters and indicators in the production process.