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The manufacturing method
of magnesium nitrate
1. Introduction
Magnesium nitrate is an important inorganic chemicals, widely used in agriculture, medicine, food, metallurgy and other fields. Therefore, it is of great practical significance to study the manufacturing method of magnesium nitrate. This article will introduce the manufacturing method of magnesium nitrate, including raw material preparation, reaction process, post-treatment and product quality control.
2. Raw Material Preparation
The manufacture of magnesium nitrate requires nitric acid and magnesium oxide as raw materials. Among them, nitric acid can be used industrial grade nitric acid, magnesium oxide is required to use high purity magnesium oxide powder. In the process of raw material preparation, the following points need to be paid attention to:
1. Control the purity of raw materials: In order to ensure product quality, high-purity magnesium oxide powder and industrial grade nitric acid are required.
2. Control the ratio of raw materials: According to the chemical formula of magnesium nitrate, the molar ratio of nitric acid to magnesium oxide should be 2:1.
3. reaction process
magnesium nitrate manufacturing using wet process, the specific steps are as follows:
1. magnesium oxide powder is added to a certain amount of water, stirring evenly, made of magnesium oxide suspension.
2. Nitric acid was slowly added to the magnesium oxide suspension while stirring to allow a sufficient reaction.
3. The pH value is controlled within a certain range during the reaction to ensure the progress of the reaction and the quality of the product.
4. After completion of the reaction, the reaction mixture was filtered, washed and dried to obtain a magnesium nitrate product.
During the reaction process, the following points need to be paid attention to:
1. Control the acid addition speed: Too fast acid addition speed will cause local peracid and affect product quality.
2. Control the reaction temperature: Too high reaction temperature will cause product decomposition and affect product quality.
3. Control pH: Too high or too low pH will affect the purity and yield of the product.
4. post-treatment
After the
reaction is completed, the product needs to be post-treated, including filtering, washing, drying and other steps. In these steps, the following points need to be paid attention to:
1. Filtration: Use appropriate filtration equipment to ensure product purity.
2. Washing: Washing the product with pure water to remove impurities.
3. Drying: Use appropriate drying equipment to control the drying temperature and time to ensure product quality.
5. product quality control
In order to ensure the quality of magnesium nitrate products, it is necessary to control the quality of products, including purity, particle size, water content and other aspects of the detection. In these tests, the following points need to be paid attention to:
1. Purity test: Use appropriate analytical methods, such as titration, spectroscopy, etc., to detect the purity of magnesium nitrate in the product.
2. Particle size detection: use particle size analyzer and other equipment to detect the particle size distribution of the product to ensure the fluidity and performance of the product.
3. Water content detection: The method of loss on drying is used to detect the water content of the product to ensure the stability and service life of the product.
6. conclusion The manufacturing method of
magnesium nitrate includes raw material preparation, reaction process, post-treatment and product quality control. In the manufacturing process, it is necessary to strictly control factors such as raw material purity, ratio, reaction conditions, post-treatment process and product quality to ensure product quality and yield. At the same time, it is necessary to select appropriate equipment and processes according to the actual situation to improve production efficiency and economic benefits.