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Manufacturing method
of manganese carbonate
1. Introduction
manganese carbonate as an important inorganic chemicals, widely used in metallurgy, ceramics, glass, fertilizer and other fields. Especially in the metallurgical industry, manganese carbonate is often used as a raw material for smelting ferromanganese alloy and manufacturing manganese metal. In this paper, the manufacturing method of manganese carbonate is discussed in detail.
2. raw materials and equipment
1. raw materials: the main raw materials for the preparation of manganese carbonate manganese ore, sulfuric acid and carbonate. Among them, the higher the content of manganese in manganese ore, the higher the purity of the prepared manganese carbonate.
2. Equipment: The required equipment includes crusher, ball mill, stirred reactor, centrifuge, dryer, etc.
3. manufacturing methods
1. Crushing and grinding of manganese ore: Crushing and grinding of manganese ore to make its particle size reach a certain fineness, so as to increase the surface area of manganese ore and improve the reaction rate.
2. Acid leaching: the manganese ore after grinding is mixed with sulfuric acid in a certain proportion, and the reaction is carried out in a stirred reactor to convert the manganese in the manganese ore into manganese sulfate. It is necessary to control the concentration of sulfuric acid and the reaction temperature during the reaction to ensure the smooth progress of the reaction.
3. Neutralization: mixing manganese sulfate solution with carbonate solution, neutralization reaction occurs, and manganese carbonate precipitate is generated. In this process, the pH value needs to be controlled to ensure the purity of manganese carbonate.
4. Centrifugation: The manganese carbonate precipitate was separated from the mother liquor by a centrifuge, and the manganese carbonate precipitate was collected.
5. Washing and drying: The manganese carbonate precipitate is washed with deionized water to remove impurity ions attached to the surface, and then the washed manganese carbonate precipitate is dried to obtain a manganese carbonate product.
4. precautions
1. In the acid leaching process, it is necessary to pay attention to the concentration and temperature control of sulfuric acid to avoid excessive acidity and temperature corrosion and loss of equipment.
2. During the neutralization process, the pH value needs to be strictly controlled to ensure the purity of the generated manganese carbonate. At the same time, attention needs to be paid to the choice of carbonate to avoid introducing new impurities.
3. In the centrifugal separation process, it is necessary to ensure the speed and time of the centrifuge to ensure the effective separation of the manganese carbonate precipitate and the mother liquor.
4. In the process of washing and drying, it is necessary to pay attention to the selection of water consumption and water quality to avoid incomplete washing or incomplete drying and affecting product quality.
5. conclusion The manufacturing method of
manganese carbonate mainly includes the crushing and grinding of manganese ore, acid leaching, neutralization, centrifugal separation, washing and drying steps. In the manufacturing process, attention should be paid to the selection of raw materials, equipment maintenance and operation control to ensure product quality and production efficiency. Through the continuous optimization and improvement of the manufacturing method, the purity and yield of manganese carbonate can be further improved, and better raw material guarantee can be provided for related industries.