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Source:Transform the World with Simplicity
MIBK (methyl isobutyl ketone) is an important chemical raw material, widely used in solvents, pharmaceuticals, pesticides, spices and other fields. This article will introduce the manufacturing method of MIBK, including raw material preparation, reaction process, post-treatment and so on.
1. Feedstock Preparation
The main feedstocks for the manufacture of MIBK are isobutylene and methanol. Isobutene can be obtained by naphtha cracking, propylene disproportionation, etc., and methanol can be obtained by syngas synthesis or natural gas preparation. In the process of raw material preparation, it is necessary to ensure the purity and quality of raw materials to avoid adverse effects on subsequent reactions.
2. Reaction Process
The manufacture of MIBK is primarily obtained by the ketonization of isobutene and methanol. The ketonization reaction is an acid-catalyzed reaction, and commonly used catalysts include sulfuric acid, phosphoric acid, etc. During the reaction, the reaction temperature, pressure and the amount of catalyst need to be controlled to ensure the smooth progress of the reaction and the purity of the product. At the same time, it is also necessary to adjust the pH value and dehydrate the reaction solution to avoid by-products and affect the quality of the product.
3. post-treatment
After the reaction is completed, the reaction solution needs to be subjected to post-treatment such as separation and distillation to obtain MIBK products with high purity. In the post-processing process, it is necessary to pay attention to control the quality and yield of the product to avoid waste and loss. At the same time, it is also necessary to properly dispose of waste to avoid pollution to the environment.
In short, the manufacture of MIBK needs to go through multiple links such as raw material preparation, reaction process and post-treatment, and it is necessary to strictly control the operating conditions and parameters of each link to ensure the quality and yield of the product. At the same time, it is also necessary to pay attention to safety production and environmental protection requirements to ensure the smooth progress of the production process and minimize the impact on the environment.